Professor SAM KINGMAN's Outputs (12)

Towards sustainable processing of columbite group minerals: Elucidating the relation between dielectric properties and physico-chemical transformations in the mineral phase (2017)
Journal Article
Sanchez-Segado, S., Monti, T., Katrib, J., Kingman, S., Dodds, C., & Jha, A. (2017). Towards sustainable processing of columbite group minerals: Elucidating the relation between dielectric properties and physico-chemical transformations in the mineral phase. Scientific Reports, 7(1), Article 18016. https://doi.org/10.1038/s41598-017-18272-3

© 2017 The Author(s). Current methodologies for the extraction of tantalum and niobium pose a serious threat to human beings and the environment due to the use of hydrofluoric acid (HF). Niobium and tantalum metal powders and pentoxides are widely us... Read More about Towards sustainable processing of columbite group minerals: Elucidating the relation between dielectric properties and physico-chemical transformations in the mineral phase.

Thermal analysis on the pyrolysis of tetrabromobisphenol A (TBBPA) and Electric Arc Furnace Dust mixtures (2017)
Journal Article
Al-Harahsheh, M., Al-Otoom, A., Al-Jarrah, M., Altarawneh, M., & Kingman, S. (in press). Thermal analysis on the pyrolysis of tetrabromobisphenol A (TBBPA) and Electric Arc Furnace Dust mixtures. Metallurgical and Materials Transactions B, 49(1), https://doi.org/10.1007/s11663-017-1121-7

The pyrolysis of Tetrabromobisphenol A (TBBPA) mixed with Electric Arc Furnace Dust (EAFD) was studied using thermogravimetric analysis (TGA) and theoretically analysed using thermodynamic equilibrium calculations. Mixtures of both materials with var... Read More about Thermal analysis on the pyrolysis of tetrabromobisphenol A (TBBPA) and Electric Arc Furnace Dust mixtures.

Microwave treatment of electric arc furnace dust with Tetrabromobisphenol A: Dielectric characterization and pyrolysis-leaching (2017)
Journal Article
Al-Harahsheh, M., Kingman, S., & Hamilton, I. S. (2017). Microwave treatment of electric arc furnace dust with Tetrabromobisphenol A: Dielectric characterization and pyrolysis-leaching. Journal of Analytical and Applied Pyrolysis, 128, https://doi.org/10.1016/j.jaap.2017.10.013

In the present work microwave treatment of electric arc furnace dust (EAFD) mixed with tetrabromobisphenol A (TBBPA) was investigated. A range of characterization techniques were used to understand the thermal behaviour of TBBPA-EAFD mixtures under m... Read More about Microwave treatment of electric arc furnace dust with Tetrabromobisphenol A: Dielectric characterization and pyrolysis-leaching.

Benefits of dry comminution of biomass pellets in a knife mill (2017)
Journal Article
Williams, O., Lester, E., Kingman, S., Giddings, D., Lormor, S., & Eastwick, C. (in press). Benefits of dry comminution of biomass pellets in a knife mill. Biosystems Engineering, 160, https://doi.org/10.1016/j.biosystemseng.2017.05.011

The potential benefits of dry comminution in a knife mill for a diverse range of biomass 6 pellets are explored. The impact of dry comminution on energy consumption, particle size and shape, 7 is examined as well as the link between milling and mecha... Read More about Benefits of dry comminution of biomass pellets in a knife mill.

Towards large scale microwave treatment of ores: Part 2 - Metallurgical testing (2017)
Journal Article
Batchelor, A., Buttress, A., Jones, D., Katrib, J., Way, D., Chenje, T., Stoll, D., Dodds, C., & Kingman, S. (2017). Towards large scale microwave treatment of ores: Part 2 - Metallurgical testing. Minerals Engineering, 111, 5-24. https://doi.org/10.1016/j.mineng.2017.05.003

© 2017 A pilot scale microwave treatment system capable of treating 10–150t/h of material at 10–200kW was designed, constructed and commissioned in order to understand the engineering challenges of microwave-induced fracture of ores at scale and gene... Read More about Towards large scale microwave treatment of ores: Part 2 - Metallurgical testing.

Microwave fluidized bed for biomass pyrolysis. Part II: Effect of process parameters (2017)
Journal Article
Adam, M., Beneroso, D., Katrib, J., Kingman, S., & Robinson, J. P. (in press). Microwave fluidized bed for biomass pyrolysis. Part II: Effect of process parameters. Biofuels, Bioproducts and Biorefining, https://doi.org/10.1002/bbb.1781

The microwave fluidized bed process developed in Part I (DOI: 10.1002/bbb.1780), in which the heating heterogeneity issues are overcome, has been applied to the pyrolysis of biomass. The degree of pyrolysis was established by studying the behavior of... Read More about Microwave fluidized bed for biomass pyrolysis. Part II: Effect of process parameters.

Microwave fluidized bed for biomass pyrolysis. Part I: Process design (2017)
Journal Article
Adam, M., Beneroso, D., Katrib, J., Kingman, S., & Robinson, J. P. (in press). Microwave fluidized bed for biomass pyrolysis. Part I: Process design. Biofuels, Bioproducts and Biorefining, https://doi.org/10.1002/bbb.1780

The production of bio-oils from microwave pyrolysis has received increasing attention from bioenergy researchers, but no studies reported to date have proposed reliable solutions to avoid thermal runaway. The motivation of this paper is to develop an... Read More about Microwave fluidized bed for biomass pyrolysis. Part I: Process design.

Towards large scale microwave treatment of ores: Part 1 – Basis of design, construction and commissioning (2017)
Journal Article
Buttress, A., Katrib, J., Batchelor, A., Jones, D., Craig, D., Royal, T., Dodds, C., & Kingman, S. (2017). Towards large scale microwave treatment of ores: Part 1 – Basis of design, construction and commissioning. Minerals Engineering, 109, https://doi.org/10.1016/j.mineng.2017.03.006

Despite over thirty years of work, microwave pre-treatment processes for beneficiation of ores have not progressed much further than laboratory testing. In this paper we present a scaleable pilot-scale system for the microwave treatment of ores capab... Read More about Towards large scale microwave treatment of ores: Part 1 – Basis of design, construction and commissioning.

Metal-organic frameworks in seconds via selective microwave heating (2017)
Journal Article
Laybourn, A., Katrib, J., Ferrari-John, R. S., Morris, C. G., Yang, S., Udoudo, O., Easun, T. L., Dodds, C., Champness, N. R., Kingman, S. W., & Schröder, M. (2017). Metal-organic frameworks in seconds via selective microwave heating. Journal of Materials Chemistry A, 5(16), 7333-7338. https://doi.org/10.1039/C7TA01493G

© The Royal Society of Chemistry. Synthesis of metal-organic framework (MOF) materials via microwave heating often involves shorter reaction times and offers enhanced control of particle size compared to conventional heating. However, there is little... Read More about Metal-organic frameworks in seconds via selective microwave heating.

Overcoming the caking phenomenon in olive mill wastes (2017)
Journal Article
Williams, O., Eastwick, C., Kingman, S., Giddings, D., Lormor, S., & Lester, E. (2017). Overcoming the caking phenomenon in olive mill wastes. Industrial Crops and Products, 101, https://doi.org/10.1016/j.indcrop.2017.02.036

The use of olive mill wastes (orujillo) within coal fired power stations in the UK has led to unexpected difficulties with material caking within the fuel handling plant. This study replicated orujillo caking on a laboratory scale using a planetary b... Read More about Overcoming the caking phenomenon in olive mill wastes.

New insights into microwave pyrolysis of biomass: preparation of carbon-based products from pecan nutshells and their application in wastewater treatment (2017)
Journal Article
Duran Jimenez, G., Monti, T., Titman, J. J., Hernandez-Montoya, V., Kingman, S., & Binner, E. (2017). New insights into microwave pyrolysis of biomass: preparation of carbon-based products from pecan nutshells and their application in wastewater treatment. Journal of Analytical and Applied Pyrolysis, 124, https://doi.org/10.1016/j.jaap.2017.02.013

Microwave pyrolysis of pecan nutshell (Carya illinoinensis) biomass was used to produce carbon-based solid products with potential application in contaminated water treatment.

A range of analytical techniques were applied to characterize the inter... Read More about New insights into microwave pyrolysis of biomass: preparation of carbon-based products from pecan nutshells and their application in wastewater treatment.

Statistical description of inhomogeneous samples by scanning microwave microscopy (2017)
Journal Article
Monti, T., Udoudo, O., Sperin, K. A., Dodds, C., Kingman, S., & Jackson, T. J. (2017). Statistical description of inhomogeneous samples by scanning microwave microscopy. IEEE Transactions on Microwave Theory and Techniques, 65(6), https://doi.org/10.1109/TMTT.2016.2642940

A quantitative analysis of the dielectric properties of a multiphase sample using a scanning microwave microscope (SMM) is proposed. The method is demonstrated using inhomogeneous samples composed of a resin containing micrometric inclusions of a kno... Read More about Statistical description of inhomogeneous samples by scanning microwave microscopy.