Skip to main content

Research Repository

See what's under the surface

Advanced Search

Continuous synthesis of Zn2Al-CO3 layered double hydroxides: A comparison of bench, pilot and industrial scale syntheses

Clark, I.; Gomes, R. L.; Crawshaw, C.; Neve, L.; Lodge, R.; Fay, M.; Winkler, C.; Hull, M.; Lester, E.

Authors

I. Clark

R. L. Gomes

C. Crawshaw

L. Neve

R. Lodge

C. Winkler

M. Hull

E. Lester



Abstract

© 2019 The Royal Society of Chemistry. Zn2Al-CO3 was produced continuously at bench (g h-1), pilot (100s g h-1) and industrial scale (10s kg h-1). Crystal domain length and BET surface area were similar at all three scales although there was a small increase at pilot scale. Platelet size increased from 120 nm at bench to 177 nm and 165 nm at pilot scale and industrial scale, respectively. Overall this paper shows that the increase in scale by almost 2000× does not impact on the overall product quality which is an excellent indicator that continuous hydrothermal synthesis is a route for nanomaterials synthesis.

Journal Article Type Article
Publication Date Apr 1, 2019
Journal Reaction Chemistry and Engineering
Electronic ISSN 2058-9883
Publisher Royal Society of Chemistry
Peer Reviewed Peer Reviewed
Volume 4
Issue 4
Pages 663-666
APA6 Citation Clark, I., Gomes, R. L., Crawshaw, C., Neve, L., Lodge, R., Fay, M., …Lester, E. (2019). Continuous synthesis of Zn2Al-CO3 layered double hydroxides: A comparison of bench, pilot and industrial scale syntheses. Reaction Chemistry and Engineering, 4(4), 663-666. https://doi.org/10.1039/c8re00241j
DOI https://doi.org/10.1039/c8re00241j
Publisher URL https://pubs.rsc.org/en/content/articlelanding/2019/re/c8re00241j#!divAbstract
Additional Information : This document is Similarity Check deposited; : Supplementary Information; : I. Clark (ORCID); : R. L. Gomes (ORCID); : R. L. Gomes (ResearcherID); : R. Lodge (ORCID); : M. Fay (ORCID); : E. Lester (ORCID); : Single-blind; : Received 3 October 2018; Accepted 4 December 2018; Advance Article published 8 March 2019; Version of Record published 26 March 2019

Files

Continuous synthesis of Zn2Al–CO3 layered double hydroxides: a comparison of bench, pilot and industrial scale syntheses (1.7 Mb)
PDF





You might also like



Downloadable Citations

;