Skip to main content

Research Repository

Advanced Search

All Outputs (10)

Towards sustainable processing of columbite group minerals: Elucidating the relation between dielectric properties and physico-chemical transformations in the mineral phase (2017)
Journal Article
Sanchez-Segado, S., Monti, T., Katrib, J., Kingman, S., Dodds, C., & Jha, A. (2017). Towards sustainable processing of columbite group minerals: Elucidating the relation between dielectric properties and physico-chemical transformations in the mineral phase. Scientific Reports, 7(1), Article 18016. https://doi.org/10.1038/s41598-017-18272-3

© 2017 The Author(s). Current methodologies for the extraction of tantalum and niobium pose a serious threat to human beings and the environment due to the use of hydrofluoric acid (HF). Niobium and tantalum metal powders and pentoxides are widely us... Read More about Towards sustainable processing of columbite group minerals: Elucidating the relation between dielectric properties and physico-chemical transformations in the mineral phase.

Selective molecular annealing: in situ small angle X-ray scattering study of microwave-assisted annealing of block copolymers (2017)
Journal Article
Toolan, D. T., Adlington, K., Isakova, A., Kalamiotis, A., Mokarian-Tabari, P., Dimitrakis, G., …Howse, J. R. (2017). Selective molecular annealing: in situ small angle X-ray scattering study of microwave-assisted annealing of block copolymers. Physical Chemistry Chemical Physics, 19(31), 20412--20419. https://doi.org/10.1039/c7cp03578k

Microwave annealing has emerged as an alternative to traditional thermal annealing approaches for optimising block copolymer self-assembly. A novel sample environment enabling small angle X-ray scattering to be performed in situ during microwave anne... Read More about Selective molecular annealing: in situ small angle X-ray scattering study of microwave-assisted annealing of block copolymers.

Microwave assisted hydro-distillation of essential oils from fresh ginger root (Zingiber officinale Roscoe) (2017)
Journal Article
Racoti, A., Buttress, A., Binner, E., Dodds, C., Trifan, A., & Calinescu, I. (2017). Microwave assisted hydro-distillation of essential oils from fresh ginger root (Zingiber officinale Roscoe). Journal of Essential Oil Research, https://doi.org/10.1080/10412905.2017.1360216

A solvent free in situ microwave hydro-distillation method for extraction of essential oil from fresh ginger root it presented. Extraction was conducted in a TE10n single-mode microwave cavity and variable power 2 kW generator operating at 2.45GHz. T... Read More about Microwave assisted hydro-distillation of essential oils from fresh ginger root (Zingiber officinale Roscoe).

Towards large scale microwave treatment of ores: Part 2 - Metallurgical testing (2017)
Journal Article
Batchelor, A., Buttress, A., Jones, D., Katrib, J., Way, D., Chenje, T., …Kingman, S. (2017). Towards large scale microwave treatment of ores: Part 2 - Metallurgical testing. Minerals Engineering, 111, 5-24. https://doi.org/10.1016/j.mineng.2017.05.003

© 2017 A pilot scale microwave treatment system capable of treating 10–150t/h of material at 10–200kW was designed, constructed and commissioned in order to understand the engineering challenges of microwave-induced fracture of ores at scale and gene... Read More about Towards large scale microwave treatment of ores: Part 2 - Metallurgical testing.

Calibrated X-ray micro-tomography for mineral ore quantification (2017)
Journal Article
Reyes, F., Lin, Q., Udoudo, O., Dodds, C., Lee, P., & Neethling, S. (2017). Calibrated X-ray micro-tomography for mineral ore quantification. Minerals Engineering, 110, https://doi.org/10.1016/j.mineng.2017.04.015

Scanning Electron Microscopy (SEM) based assessments are the most widely used and trusted imaging technique for mineral ore quantification. X-ray micro tomography (XMT) is a more recent addition to the mineralogy toolbox, but with the potential to ex... Read More about Calibrated X-ray micro-tomography for mineral ore quantification.

Towards large scale microwave treatment of ores: Part 1 – Basis of design, construction and commissioning (2017)
Journal Article
Buttress, A., Katrib, J., Batchelor, A., Jones, D., Craig, D., Royal, T., …Kingman, S. (2017). Towards large scale microwave treatment of ores: Part 1 – Basis of design, construction and commissioning. Minerals Engineering, 109, https://doi.org/10.1016/j.mineng.2017.03.006

Despite over thirty years of work, microwave pre-treatment processes for beneficiation of ores have not progressed much further than laboratory testing. In this paper we present a scaleable pilot-scale system for the microwave treatment of ores capab... Read More about Towards large scale microwave treatment of ores: Part 1 – Basis of design, construction and commissioning.

Metal-organic frameworks in seconds via selective microwave heating (2017)
Journal Article
Laybourn, A., Katrib, J., Ferrari-John, R. S., Morris, C. G., Yang, S., Udoudo, O., …Schröder, M. (2017). Metal-organic frameworks in seconds via selective microwave heating. Journal of Materials Chemistry A, 5(16), 7333-7338. https://doi.org/10.1039/C7TA01493G

© The Royal Society of Chemistry. Synthesis of metal-organic framework (MOF) materials via microwave heating often involves shorter reaction times and offers enhanced control of particle size compared to conventional heating. However, there is little... Read More about Metal-organic frameworks in seconds via selective microwave heating.

New insights into the role of selective and volumetric heating during microwave extraction: investigation of the extraction of polyphenolic compounds from sea buckthorn leaves using microwave-assisted extraction and conventional solvent extraction (2017)
Journal Article
Galan, A., Calinescu, I., Trifan, A., Winkworth-Smith, C., Calvo-Carrascal, M., Dodds, C., & Binner, E. (2017). New insights into the role of selective and volumetric heating during microwave extraction: investigation of the extraction of polyphenolic compounds from sea buckthorn leaves using microwave-assisted extraction and conventional solvent extraction. Chemical Engineering and Processing: Process Intensification, 116, 29-39. https://doi.org/10.1016/j.cep.2017.03.006

We report a direct comparison of microwave heating and conventional heating in solvent extraction by using exactly the same reaction conditions (including heating rate) in the extraction of polyphenols from dried sea buckthorn leaves. We have for the... Read More about New insights into the role of selective and volumetric heating during microwave extraction: investigation of the extraction of polyphenolic compounds from sea buckthorn leaves using microwave-assisted extraction and conventional solvent extraction.

Statistical description of inhomogeneous samples by scanning microwave microscopy (2017)
Journal Article
Monti, T., Udoudo, O., Sperin, K. A., Dodds, C., Kingman, S., & Jackson, T. J. (2017). Statistical description of inhomogeneous samples by scanning microwave microscopy. IEEE Transactions on Microwave Theory and Techniques, 65(6), https://doi.org/10.1109/TMTT.2016.2642940

A quantitative analysis of the dielectric properties of a multiphase sample using a scanning microwave microscope (SMM) is proposed. The method is demonstrated using inhomogeneous samples composed of a resin containing micrometric inclusions of a kno... Read More about Statistical description of inhomogeneous samples by scanning microwave microscopy.