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The interaction of volatile metal coatings during the laser powder bed fusion of copper (2021)
Journal Article
Speidel, A., Wadge, M. D., Gargalis, L., Cooper, T. P., Reynolds, W., Grant, D., …Murray, J. W. (2022). The interaction of volatile metal coatings during the laser powder bed fusion of copper. Journal of Materials Processing Technology, 299, Article 117332. https://doi.org/10.1016/j.jmatprotec.2021.117332

The high optical reflectance of Cu at near-infrared wavelengths narrows the process window to fabricate Cu parts by laser powder bed fusion (LPBF). Coating powders with optically absorptive materials has been investigated to improve processability an... Read More about The interaction of volatile metal coatings during the laser powder bed fusion of copper.

Bespoke 3D-Printed Polydrug Implants Created via Microstructural Control of Oligomers (2021)
Journal Article
Ruiz-Cantu, L., Trindade, G. F., Taresco, V., Zhou, Z., He, Y., Burroughs, L., …Wildman, R. D. (2021). Bespoke 3D-Printed Polydrug Implants Created via Microstructural Control of Oligomers. ACS Applied Materials and Interfaces, 13(33), 38969-38978. https://doi.org/10.1021/acsami.1c07850

Controlling the microstructure of materials by means of phase separation is a versatile tool for optimizing material properties. Phase separation has been exploited to fabricate intricate microstructures in many fields including cell biology, tissue... Read More about Bespoke 3D-Printed Polydrug Implants Created via Microstructural Control of Oligomers.

Process-structure-property relationships in laser powder bed fusion of permanent magnetic Nd-Fe-B (2021)
Journal Article
Wu, J., Aboulkhair, N. T., Degano, M., Ashcroft, I., & Hague, R. J. (2021). Process-structure-property relationships in laser powder bed fusion of permanent magnetic Nd-Fe-B. Materials and Design, 209, Article 109992. https://doi.org/10.1016/j.matdes.2021.109992

Laser powder-bed fusion (L-PBF), as an additive manufacturing (AM) technique, has demonstrated excellent capabilities in achieving degrees of freedom in manufacturing that are otherwise unattainable. The potential of combining Nd-Fe-B as a permanent... Read More about Process-structure-property relationships in laser powder bed fusion of permanent magnetic Nd-Fe-B.

Modelling the influence of UV curing strategies for optimisation of inkjet based 3D printing (2021)
Journal Article
Zhao, P., He, Y., Trindade, G. F., Baumers, M., Irvine, D., Hague, R., …Wildman Conceptualisation, R. (2021). Modelling the influence of UV curing strategies for optimisation of inkjet based 3D printing. Materials and Design, 208, Article 109889. https://doi.org/10.1016/j.matdes.2021.109889

A predictive model is developed to assist in the design and manufacture of structures by inkjet based 3D printing (IJ3DP)/additive manufacturing. IJ3DP often exploits photopolymerisation to rapidly convert a photoreactive liquid ink into a solid prod... Read More about Modelling the influence of UV curing strategies for optimisation of inkjet based 3D printing.

Exploiting Generative Design for 3D Printing of Bacterial Biofilm Resistant Composite Devices (2021)
Journal Article
He, Y., Abdi, M., Trindade, G. F., Begines, B., Dubern, J. F., Prina, E., …Wildman, R. D. (2021). Exploiting Generative Design for 3D Printing of Bacterial Biofilm Resistant Composite Devices. Advanced Science, 8(15), Article 2100249. https://doi.org/10.1002/advs.202100249

As the understanding of disease grows, so does the opportunity for personalization of therapies targeted to the needs of the individual. To bring about a step change in the personalization of medical devices it is shown that multi-material inkjet-bas... Read More about Exploiting Generative Design for 3D Printing of Bacterial Biofilm Resistant Composite Devices.

Residual polymer stabiliser causes anisotropic electrical conductivity during inkjet printing of metal nanoparticles (2021)
Journal Article
Trindade, G. F., Wang, F., Im, J., He, Y., Balogh, A., Scurr, D., …Roberts, C. J. (2021). Residual polymer stabiliser causes anisotropic electrical conductivity during inkjet printing of metal nanoparticles. Communications Materials, 2(1), Article 47. https://doi.org/10.1038/s43246-021-00151-0

Inkjet printing of metal nanoparticles allows for design flexibility, rapid processing and enables the 3D printing of functional electronic devices through co-deposition of multiple materials. However, the performance of printed devices, especially t... Read More about Residual polymer stabiliser causes anisotropic electrical conductivity during inkjet printing of metal nanoparticles.

Microstructure and tensile properties of additive manufactured Ti-6Al-4V with refined prior-? grain structure obtained by rapid heat treatment (2021)
Journal Article
Zou, Z., Simonelli, M., Katrib, J., Dimitrakis, G., & Hague, R. (2021). Microstructure and tensile properties of additive manufactured Ti-6Al-4V with refined prior-? grain structure obtained by rapid heat treatment. Materials Science and Engineering: A, 814, Article 141271. https://doi.org/10.1016/j.msea.2021.141271

Heat treatments tailored for additive manufactured Ti-6Al-4V can be used to attain desirable microstructures associated with superior mechanical properties. Rapid heat treatments, for example, can be used to recrystallise the microstructure of laser... Read More about Microstructure and tensile properties of additive manufactured Ti-6Al-4V with refined prior-? grain structure obtained by rapid heat treatment.

UV-curable silicone materials with tuneable mechanical properties for 3D Printing (2021)
Journal Article
Foerster, A., Annarasa, V., Terry, A., Wildman, R., Hague, R., Irvine, D., …Tuck, C. (2021). UV-curable silicone materials with tuneable mechanical properties for 3D Printing. Materials and Design, Article 109681. https://doi.org/10.1016/j.matdes.2021.109681

In this paper, we present the development of a family of novel, UV-curable, highly flexible, 3D printable silicone-based materials, the mechanical properties of which can be tuned simply by varying the ratio of the polymerisable reagents within the f... Read More about UV-curable silicone materials with tuneable mechanical properties for 3D Printing.

Modulating the biological function of protein by tailoring the adsorption orientation on nanoparticles (2020)
Journal Article
Jain, A., Trindade, G. F., Hicks, J. M., Potts, J. C., Rahman, R., J. M. Hague, R., …Rawson, F. J. (2021). Modulating the biological function of protein by tailoring the adsorption orientation on nanoparticles. Journal of Colloid and Interface Science, 587, 150-161. https://doi.org/10.1016/j.jcis.2020.12.025

Protein orientation in nanoparticle-protein conjugates plays a crucial role in binding to cell receptors and ultimately, defines their targeting efficiency. Therefore, understanding fundamental aspects of the role of protein orientation upon adsorpti... Read More about Modulating the biological function of protein by tailoring the adsorption orientation on nanoparticles.

Additive Manufacturing and Testing of a Soft Magnetic Rotor for a Switched Reluctance Motor (2020)
Journal Article
Gargalis, L., Madonna, V., Giangrande, P., Rocca, R., Hardy, M., Ashcroft, I., …Hague, R. (2020). Additive Manufacturing and Testing of a Soft Magnetic Rotor for a Switched Reluctance Motor. IEEE Access, 8, 206982-206991. https://doi.org/10.1109/ACCESS.2020.3037190

Additive manufacturing is acknowledged as a key enabling technology, although its adoption is still constrained to niche applications. A promising area for this technology is the production of electrical machines (EMs) and/or their main components (e... Read More about Additive Manufacturing and Testing of a Soft Magnetic Rotor for a Switched Reluctance Motor.

Inter-Flake Quantum Transport of Electrons and Holes in Inkjet-Printed Graphene Devices (2020)
Journal Article
Wang, F., Gosling, J. H., Rance, G. A., Trindade, G. F., Makarovsky, O., Cottam, N. D., …Turyanska, L. (2021). Inter-Flake Quantum Transport of Electrons and Holes in Inkjet-Printed Graphene Devices. Advanced Functional Materials, 31(5), Article 2007478. https://doi.org/10.1002/adfm.202007478

© 2020 The Authors. Advanced Functional Materials published by Wiley-VCH GmbH 2D materials have unique structural and electronic properties with potential for transformative device applications. However, such devices are usually bespoke structures ma... Read More about Inter-Flake Quantum Transport of Electrons and Holes in Inkjet-Printed Graphene Devices.

Recommended Personal Protective Equipment for Cochlear Implant and Other Mastoid Surgery During the COVID-19 Era (2020)
Journal Article
Lawrence, R. J., O'Donoghue, G., Kitterick, P., O'Donoghue, K., Hague, R., Mitchell, L., …Hartley, D. E. (2020). Recommended Personal Protective Equipment for Cochlear Implant and Other Mastoid Surgery During the COVID-19 Era. Laryngoscope, 130(11), 2693-2699. https://doi.org/10.1002/lary.29014

© 2020 American Laryngological, Rhinological and Otological Society Inc, "The Triological Society" and American Laryngological Association (ALA) Objectives/Hypothesis: The overall aim of this study was to evaluate personal protective equipment (PPE)... Read More about Recommended Personal Protective Equipment for Cochlear Implant and Other Mastoid Surgery During the COVID-19 Era.

Generation of graded porous structures by control of process parameters in the selective laser melting of a fixed ratio salt-metal feedstock (2020)
Journal Article
Aboulkhair, N. T., Zhao, G., Hague, R. J., Kennedy, A. R., Ashcroft, I. A., & Clare, A. T. (2020). Generation of graded porous structures by control of process parameters in the selective laser melting of a fixed ratio salt-metal feedstock. Journal of Manufacturing Processes, 55, 249-253. https://doi.org/10.1016/j.jmapro.2020.04.039

The demonstration of salt dissolution incorporated within laser powder-bed fusion fabrication processes has allowed the creation of complex porous structures without the need for sophisticated design algorithms. This serves to simplify the process, f... Read More about Generation of graded porous structures by control of process parameters in the selective laser melting of a fixed ratio salt-metal feedstock.

The Influence of Iron in Minimizing the Microstructural Anisotropy of Ti-6Al-4V Produced by Laser Powder-Bed Fusion (2020)
Journal Article
Simonelli, M., McCartney, D. G., Barriobero-Vila, P., Aboulkhair, N. T., Tse, Y. Y., Clare, A., & Hague, R. (2020). The Influence of Iron in Minimizing the Microstructural Anisotropy of Ti-6Al-4V Produced by Laser Powder-Bed Fusion. Metallurgical and Materials Transactions A, 51, 2444–2459. https://doi.org/10.1007/s11661-020-05692-6

There remains a significant challenge in adapting alloys for metal based Additive Manufacturing (AM). Adjusting alloy composition to suit the process, particularly under regimes close to industrial practice, is therefore a potential solution. With th... Read More about The Influence of Iron in Minimizing the Microstructural Anisotropy of Ti-6Al-4V Produced by Laser Powder-Bed Fusion.

A Reactive Prodrug Ink Formulation Strategy for Inkjet 3D Printing of Controlled Release Dosage Forms and Implants (2020)
Journal Article
He, Y., Foralosso, R., Ferraz Trindade, G., Ilchev, A., Cantu, L. R., Clark, E., …Wildman, R. D. (2020). A Reactive Prodrug Ink Formulation Strategy for Inkjet 3D Printing of Controlled Release Dosage Forms and Implants. Advanced Therapeutics, 3(6), Article 1900187. https://doi.org/10.1002/adtp.201900187

We propose a strategy for creating tuneable 3D printed drug delivery devices. 3D printing offers the opportunity for improved compliance and patient treatment outcomes through personalisation, but bottlenecks include finding formulations that provide... Read More about A Reactive Prodrug Ink Formulation Strategy for Inkjet 3D Printing of Controlled Release Dosage Forms and Implants.

Refinement of the grain structure of additive manufactured titanium alloys via epitaxial recrystallization enabled by rapid heat treatment (2020)
Journal Article
Zou, Z., Simonelli, M., Katrib, J., Dimitrakis, G., & Hague, R. (2020). Refinement of the grain structure of additive manufactured titanium alloys via epitaxial recrystallization enabled by rapid heat treatment. Scripta Materialia, 180, 66-70. https://doi.org/10.1016/j.scriptamat.2020.01.027

The coarse prior-? grain structure in titanium alloys produced by additive manufacturing is associated to mechanical anisotropy and limited fatigue life. Here we report a novel methodology to refine such structure by rapid heat treatment of Ti-6Al-4V... Read More about Refinement of the grain structure of additive manufactured titanium alloys via epitaxial recrystallization enabled by rapid heat treatment.

Towards digital metal additive manufacturing via high-temperature drop-on-demand jetting (2019)
Journal Article
Simonelli, M., Aboulkhair, N., Rasa, M., East, M., Tuck, C., Wildman, R., …Hague, R. (2019). Towards digital metal additive manufacturing via high-temperature drop-on-demand jetting. Additive Manufacturing, 30, Article 100930. https://doi.org/10.1016/j.addma.2019.100930

Drop-on-demand jetting of metals offers a fully digital manufacturing approach to surpass the limitations of the current generation powder-based additive manufacturing technologies. However, research on this topic has been restricted mainly to near-n... Read More about Towards digital metal additive manufacturing via high-temperature drop-on-demand jetting.

Wireless Nanobioelectronics for Electrical Intracellular Sensing (2019)
Journal Article
Sanjuan-Alberte, P., Jain, A., Shaw, A. J., Abayzeed, S. A., Domínguez, R. F., Alea-Reyes, M. E., …Rawson, F. J. (2019). Wireless Nanobioelectronics for Electrical Intracellular Sensing. ACS Applied Nano Materials, 2(10), 6397-6408. https://doi.org/10.1021/acsanm.9b01374

For the field of bioelectronics to make an impact on healthcare, there is an urgent requirement for the development of “wireless” electronic systems to enable modulation of chemistry inside of cells. Herein we report on an intracellular wireless elec... Read More about Wireless Nanobioelectronics for Electrical Intracellular Sensing.

Evolution of carbon nanotubes and their metallurgical reactions in Al-based composites in response to laser irradiation during selective laser melting (2019)
Journal Article
Aboulkhair, N. T., Simonelli, M., Salama, E., Rance, G., Neate, N. C., Tuck, C. J., …Hague, R. J. (2019). Evolution of carbon nanotubes and their metallurgical reactions in Al-based composites in response to laser irradiation during selective laser melting. Materials Science and Engineering: A, 765, Article 138307. https://doi.org/10.1016/j.msea.2019.138307

Aluminium-based composites reinforced with carbon nanotubes are widely sought for their outstanding metallurgical and structural properties that largely depend on the manufacturing route. In this work, the process-structure-property relationship for... Read More about Evolution of carbon nanotubes and their metallurgical reactions in Al-based composites in response to laser irradiation during selective laser melting.