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Development of samarium-doped phosphate glass microspheres for internal radiotheranostic applications (2024)
Journal Article
Arjuna, A., Milborne, B., Putra, A. R., Mulyaningsih, T. R., Setiawan, H., Islam, M. T., …Ahmed, I. (2024). Development of samarium-doped phosphate glass microspheres for internal radiotheranostic applications. International Journal of Pharmaceutics, 653, Article 123919. https://doi.org/10.1016/j.ijpharm.2024.123919

Internal radiotherapy delivers radioactive sources inside the body, near to or into malignant tumours, which may be particularly effective when malignancies are not responding to external beam radiotherapy. A pure beta emitter, 90Y, is currently used... Read More about Development of samarium-doped phosphate glass microspheres for internal radiotheranostic applications.

The Use of Microspheres for Cancer Embolization Therapy: Recent Advancements and Prospective (2024)
Journal Article
Nuzulia, N. A., Mart, T., Ahmed, I., & Sari, Y. W. (2024). The Use of Microspheres for Cancer Embolization Therapy: Recent Advancements and Prospective. ACS Biomaterials Science and Engineering, https://doi.org/10.1021/acsbiomaterials.3c00659

Embolization therapy involving biomaterials has improved the therapeutic strategy for most liver cancer treatments. Developing biomaterials as embolic agents has significantly improved patients’ survival rates. Various embolic agents are present in l... Read More about The Use of Microspheres for Cancer Embolization Therapy: Recent Advancements and Prospective.

In vitro immunomodulatory effect of solid versus porous phosphate-based glass microspheres using macrophages (2023)
Journal Article
Sheela, S., AlGhalban, F. M., Ahmed, I., & Abou Neel, E. A. (2023). In vitro immunomodulatory effect of solid versus porous phosphate-based glass microspheres using macrophages. Heliyon, 9(12), e23059. https://doi.org/10.1016/j.heliyon.2023.e23059

This study aimed to investigate the immunomodulatory effect of two different forms of phosphate-based glass microspheres (solid and porous), on human macrophages. Human THP-1 monocytes were converted to M0 macrophages after being treated with 100 ng/... Read More about In vitro immunomodulatory effect of solid versus porous phosphate-based glass microspheres using macrophages.

Rapid microwave synthesis of sustainable magnetic framework composites of UTSA-16(Zn) with Fe3O4 nanoparticles for efficient CO2 capture (2023)
Journal Article
Woodliffe, J. L., Johnston, A., Fay, M., Ferrari, R., Gomes, R. L., Lester, E., …Laybourn, A. (2023). Rapid microwave synthesis of sustainable magnetic framework composites of UTSA-16(Zn) with Fe3O4 nanoparticles for efficient CO2 capture. Materials Advances, 4(11), 5838-5849. https://doi.org/10.1039/D3MA00351E

Metal-organic frameworks (MOFs) have shown excellent potential for carbon dioxide capture applications due to their high sorption capacities and selectivities. However, MOFs are typically thermally insulating, and so thermal CO2 regeneration is chall... Read More about Rapid microwave synthesis of sustainable magnetic framework composites of UTSA-16(Zn) with Fe3O4 nanoparticles for efficient CO2 capture.

Rapid synthesis of magnetic microspheres and the development of new macro-micro hierarchically porous magnetic framework composites (2023)
Journal Article
Woodliffe, J. L., Molinar-Díaz, J., Islam, M. T., Stevens, L. A., Wadge, M. D., Rance, G. A., …Laybourn, A. (2023). Rapid synthesis of magnetic microspheres and the development of new macro-micro hierarchically porous magnetic framework composites. Journal of Materials Chemistry A, 11(27), 14705-14719. https://doi.org/10.1039/D3TA01927F

Magnetic framework composites (MFCs) are a highly interesting group of materials that contain both metal–organic frameworks (MOFs) and magnetic materials. Combining the unique benefits of MOFs (tuneable natures, high surface areas) with the advantage... Read More about Rapid synthesis of magnetic microspheres and the development of new macro-micro hierarchically porous magnetic framework composites.

Tailoring absorptivity of highly reflective Ag powders by pulsed-direct current magnetron sputtering for additive manufacturing processes (2023)
Journal Article
Wadge, M. D., Lowther, M., Cooper, T. P., Reynolds, W. J., Speidel, A., Carter, L. N., …Cox, S. C. (2023). Tailoring absorptivity of highly reflective Ag powders by pulsed-direct current magnetron sputtering for additive manufacturing processes. Journal of Materials Processing Technology, 317, Article 117985. https://doi.org/10.1016/j.jmatprotec.2023.117985

Processing of highly reflective and high thermally conductive materials (Cu, Ag, etc.) by laser powder bed fusion (LPBF) is of increasing interest to broaden the range of materials that can be additively manufactured. However, these alloys are challe... Read More about Tailoring absorptivity of highly reflective Ag powders by pulsed-direct current magnetron sputtering for additive manufacturing processes.

Optimisation of the Flame Spheroidisation Process for the Rapid Manufacture of Fe3O4-Based Porous and Dense Microspheres (2023)
Journal Article
Molinar-Díaz, J., Woodliffe, J. L., Steer, E., Morley, N. A., Brown, P. D., & Ahmed, I. (2023). Optimisation of the Flame Spheroidisation Process for the Rapid Manufacture of Fe3O4-Based Porous and Dense Microspheres. Molecules, 28(6), Article 2523. https://doi.org/10.3390/molecules28062523

The rapid, single-stage, flame-spheroidisation process, as applied to varying Fe3O4:CaCO3 powder combinations, provides for the rapid production of a mixture of dense and porous ferromagnetic microspheres with homogeneous composition, high levels of... Read More about Optimisation of the Flame Spheroidisation Process for the Rapid Manufacture of Fe3O4-Based Porous and Dense Microspheres.

Production of Nano Hydroxyapatite and Mg-Whitlockite from Biowaste-Derived products via Continuous Flow Hydrothermal Synthesis: A Step towards Circular Economy (2023)
Journal Article
Nigar, F., Johnston, A. L., Smith, J., Oakley, W., Islam, M. T., Felfel, R., …Ahmed, I. (2023). Production of Nano Hydroxyapatite and Mg-Whitlockite from Biowaste-Derived products via Continuous Flow Hydrothermal Synthesis: A Step towards Circular Economy. Materials, 16(6), Article 2138. https://doi.org/10.3390/ma16062138

Biowastes from agriculture, sewage, household wastes, and industries comprise promising resources to produce biomaterials while reducing adverse environmental effects. This study focused on utilising waste-derived materials (i.e., eggshells as a calc... Read More about Production of Nano Hydroxyapatite and Mg-Whitlockite from Biowaste-Derived products via Continuous Flow Hydrothermal Synthesis: A Step towards Circular Economy.

Ferromagnetic Cytocompatible Glass-Ceramic Porous Microspheres for Magnetic Hyperthermia Applications (2023)
Journal Article
Molinar‐Díaz, J., Woodliffe, J. L., Milborne, B., Murrell, L., Islam, M. T., Steer, E., …Ahmed, I. (2023). Ferromagnetic Cytocompatible Glass-Ceramic Porous Microspheres for Magnetic Hyperthermia Applications. Advanced Materials Interfaces, 10(11), Article 2202089. https://doi.org/10.1002/admi.202202089

Highly porous, ferromagnetic glass-ceramic P40-Fe3O4 microspheres (125–212 µm) with enhanced cytocompatibility have been manufactured for the first time via a facile, rapid, single-stage flame spheroidization process. Dispersions of Fe3O4 and Ca2Fe2O... Read More about Ferromagnetic Cytocompatible Glass-Ceramic Porous Microspheres for Magnetic Hyperthermia Applications.

Nanostructured, Alkaline Titanate‐Converted, and Heat‐Treated Ti6Al4V Microspheres via Wet‐Chemical Alkaline Modification and their ORR Electrocatalytic Response (2022)
Journal Article
Wadge, M. D., Bird, M. A., Sankowski, A., Constantin, H., Fay, M. W., Cooper, T. P., …Grant, D. M. (2023). Nanostructured, Alkaline Titanate‐Converted, and Heat‐Treated Ti6Al4V Microspheres via Wet‐Chemical Alkaline Modification and their ORR Electrocatalytic Response. Advanced Materials Interfaces, 10(5), Article 2201523. https://doi.org/10.1002/admi.202201523

This study describes the chemical conversion and heat treatment of Ti6Al4V microspheres (Ti6_MS), and the resulting effects on their electrocatalytic properties. The wet-chemical conversion (5.0m NaOH, 60°C, 24h; Sample label: Ti6_TC) converts the to... Read More about Nanostructured, Alkaline Titanate‐Converted, and Heat‐Treated Ti6Al4V Microspheres via Wet‐Chemical Alkaline Modification and their ORR Electrocatalytic Response.

Developing Porous Ortho- and Pyrophosphate-Containing Glass Microspheres; Structural and Cytocompatibility Characterisation (2022)
Journal Article
Milborne, B., Murrell, L., Cardillo-Zallo, I., Titman, J., Briggs, L., Scotchford, C., …Ahmed, I. (2022). Developing Porous Ortho- and Pyrophosphate-Containing Glass Microspheres; Structural and Cytocompatibility Characterisation. Bioengineering, 9(11), Article 611. https://doi.org/10.3390/bioengineering9110611

Phosphate-based glasses (PBGs) are promising materials for bone repair and regeneration as they can be formulated to be compositionally similar to the inorganic components of bone. Alterations to the PBG formulation can be used to tailor their degrad... Read More about Developing Porous Ortho- and Pyrophosphate-Containing Glass Microspheres; Structural and Cytocompatibility Characterisation.

L-DOPA coating improved phosphate glass fibre strength and fibre/matrix interface (2022)
Journal Article
Tan, C., Rudd, C. D., Parsons, A. J., Sharmin, N., & Ahmed, I. (2022). L-DOPA coating improved phosphate glass fibre strength and fibre/matrix interface. Journal of the Mechanical Behavior of Biomedical Materials, 136, Article 105480. https://doi.org/10.1016/j.jmbbm.2022.105480

The levodopa (L-DOPA) has been reported as a promising adhesive for various materials. In this study, we utilized L-DOPA as an interfacial agent for phosphate glass fibre/polycaprolactone (PGF/PCL) composites, with the aim to enhance the interfacial... Read More about L-DOPA coating improved phosphate glass fibre strength and fibre/matrix interface.

Upcycling Glass Waste into Porous Microspheres for Wastewater Treatment Applications: Efficacy of Dye Removal (2022)
Journal Article
Samad, S. A., Arafat, A., Lester, E., & Ahmed, I. (2022). Upcycling Glass Waste into Porous Microspheres for Wastewater Treatment Applications: Efficacy of Dye Removal. Materials, 15(17), Article 5809. https://doi.org/10.3390/ma15175809

Each year about 7.6 million tons of waste glasses are landfilled without recycling, reclaiming or upcycling. Herein we have developed a solvent free upcycling method for recycled glass waste (RG) by remanufacturing it into porous recycled glass micro... Read More about Upcycling Glass Waste into Porous Microspheres for Wastewater Treatment Applications: Efficacy of Dye Removal.

Tailored Additives for Incorporation of Antibacterial Functionality Into Laser Sintered Parts (2022)
Journal Article
Wingham, J. R., Ahmed, I., Islam, M. T., Shepherd, J., & Majewski, C. (2022). Tailored Additives for Incorporation of Antibacterial Functionality Into Laser Sintered Parts. Frontiers in Biomaterials Science, 1, Article 929006. https://doi.org/10.3389/fbiom.2022.929006

Infectious disease is a major cause of death worldwide, and novel methods capable of controlling the spread of disease are in high demand. This research presents a method of producing antimicrobial microcomposites by exploiting the powder-based natur... Read More about Tailored Additives for Incorporation of Antibacterial Functionality Into Laser Sintered Parts.

Developing Highly Porous Glass Microspheres via a Single-Stage Flame Spheroidisation Process (2022)
Journal Article
Nuzulia, N. A., Islam, T., Saputra, A., Sudiro, T., Timuda, G. E., Mart, T., …Ahmed, I. (2022). Developing Highly Porous Glass Microspheres via a Single-Stage Flame Spheroidisation Process. Journal of Physics: Conference Series, 2243(1), Article 012005. https://doi.org/10.1088/1742-6596/2243/1/012005

Glass microspheres are gaining attention in bone tissue engineering due to their ability to convert into hydroxyapatite-like materials, resembling the inorganic mineral of natural bone. The morphology of glass microspheres as starting material has be... Read More about Developing Highly Porous Glass Microspheres via a Single-Stage Flame Spheroidisation Process.

Characterization of potential nanoporous sodium titanate film formation on Ti6Al4V and TiO2 microspherical substrates via wet-chemical alkaline conversion (2022)
Journal Article
Wadge, M. D., Carrington, M. J., Constantin, H., Orange, K., Greaves, J., Islam, M. T., …Grant, D. M. (2022). Characterization of potential nanoporous sodium titanate film formation on Ti6Al4V and TiO2 microspherical substrates via wet-chemical alkaline conversion. Materials Characterization, 185, Article 111760. https://doi.org/10.1016/j.matchar.2022.111760

The authors present novel insights into the formation of nanoporous, wet-chemically produced sodium titanate films onto microspherical substrates of varying composition. Microspheres of Ti6Al4V (atomised; ca. 20–50 μm), which were utilised due to the... Read More about Characterization of potential nanoporous sodium titanate film formation on Ti6Al4V and TiO2 microspherical substrates via wet-chemical alkaline conversion.

Evolution of silicate bioglass particles as porous microspheres with a view towards orthobiologics (2022)
Journal Article
Islam, M. T., Nuzulia, N. A., Macri-Pellizzeri, L., Nigar, F., Sari, Y. W., & Ahmed, I. (2022). Evolution of silicate bioglass particles as porous microspheres with a view towards orthobiologics. Journal of Biomaterials Applications, 36(8), 1427-1443. https://doi.org/10.1177/08853282211059294

Although FDA approved and clinically utilised, research on 45S5 Bioglass® and S53P4 including other bioactive glasses continues in order to advance their applicability for a range of alternate applications. For example, rendering these particles poro... Read More about Evolution of silicate bioglass particles as porous microspheres with a view towards orthobiologics.

Functionalised SiO2 modified icephobic nanocomposite electrospun membranes for outdoor electromagnetic shielding applications (2022)
Journal Article
Tas, M., Musa, U. G., Ahmed, I., Xu, F., Smartt, C., & Hou, X. (2022). Functionalised SiO2 modified icephobic nanocomposite electrospun membranes for outdoor electromagnetic shielding applications. Polymer, 240, Article 124499. https://doi.org/10.1016/j.polymer.2021.124499

Outdoor electronic equipment such as signal stations, radar units, and cellular base stations would benefit from electromagnetic interference (EMI) shielding systems, but ice accretion on the surface of these facilities often causes critical challeng... Read More about Functionalised SiO2 modified icephobic nanocomposite electrospun membranes for outdoor electromagnetic shielding applications.

Solution precursor thermal spraying of gadolinium zirconate for thermal barrier coating (2021)
Journal Article
Leng, K., Rincon Romero, A., Venturi, F., Ahmed, I., & Hussain, T. (2022). Solution precursor thermal spraying of gadolinium zirconate for thermal barrier coating. Journal of the European Ceramic Society, 42(4), 1594-1607. https://doi.org/10.1016/j.jeurceramsoc.2021.11.050

Gadolinium zirconate (GZ) is an attractive material for thermal barrier coatings (TBCs). However, a single layer GZ coating has poor thermal cycling life compared to Yttria Stabilized Zirconia (YSZ). In this study, Solution Precursor High Velocity Ox... Read More about Solution precursor thermal spraying of gadolinium zirconate for thermal barrier coating.

Long-Term Culture of Stem Cells on Phosphate-Based Glass Microspheres: Synergistic Role of Chemical Formulation and 3D Architecture (2021)
Journal Article
Gupta, D., Hossain, K. M. Z., Roe, M., Smith, E. F., Ahmed, I., Sottile, V., & Grant, D. M. (2021). Long-Term Culture of Stem Cells on Phosphate-Based Glass Microspheres: Synergistic Role of Chemical Formulation and 3D Architecture. ACS Applied Bio Materials, 4(8), 5987-6004. https://doi.org/10.1021/acsabm.1c00120

Phosphate-based glasses (PBGs) are biomaterials that degrade under physiological conditions and can be modified to release various ions depending on end applications. This study utilized slow-degrading (P45:45P2O5-16CaO-24MgO-11Na2O10 4Fe2O3, mol %)... Read More about Long-Term Culture of Stem Cells on Phosphate-Based Glass Microspheres: Synergistic Role of Chemical Formulation and 3D Architecture.