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Microwave pyrolysis of olive pomace for bio-oil and bio-char production (2019)
Journal Article
Williams, O. S., Kostas, E. T., Durán-Jiménez, G., Shepherd, B. J., Meredith, W., Stevens, L. A., …Lye, G. J. (2020). Microwave pyrolysis of olive pomace for bio-oil and bio-char production. Chemical Engineering Journal, 387, Article 123404. https://doi.org/10.1016/j.cej.2019.123404

Olive pomace is a widely available agro-industrial waste residue in Europe that has the potential to contribute towards a circular, low carbon bio-economy. This study demonstrated, for the first time, the ability to successfully pyrolyse olive pomace... Read More about Microwave pyrolysis of olive pomace for bio-oil and bio-char production.

Pore structural evolution of shale following thermochemical treatment (2019)
Journal Article
Rigby, S. P., Jahan, H., Stevens, L., Uguna, C., Snape, C., Macnaughton, B., …Fletcher, R. S. (2020). Pore structural evolution of shale following thermochemical treatment. Marine and Petroleum Geology, 112, Article 104058. https://doi.org/10.1016/j.marpetgeo.2019.104058

Shales experience heat treatment concurrent with the presence of water or steam during reservoir engineering interventions, such as high pressure water fracking and in-situ combustion of hydrocarbons. This work utilises a novel technique, which is a... Read More about Pore structural evolution of shale following thermochemical treatment.

Mesocellular silica foam supported polyamine adsorbents for dry CO2 scrubbing: Performance of single versus blended polyamines for impregnation (2019)
Journal Article
Liu, X., Zhou, K., Farndon, M., Meier, E., Stevens, L., Liu, H., & Sun, C. (2019). Mesocellular silica foam supported polyamine adsorbents for dry CO2 scrubbing: Performance of single versus blended polyamines for impregnation. Applied Energy, 255, https://doi.org/10.1016/j.apenergy.2019.113643

© 2019 Elsevier Ltd Siliceous foams with three-dimensional mesoporous structures were synthesised and used to prepare polyethyleneimine (PEI) and tetraethylenepentamine (TEPA)-functionalised sorbent materials for CO2 capture, with a particular focus... Read More about Mesocellular silica foam supported polyamine adsorbents for dry CO2 scrubbing: Performance of single versus blended polyamines for impregnation.

Shale gas reserve evaluation by laboratory pyrolysis and gas holding capacity consistent with field data (2019)
Journal Article
Whitelaw, P., Uguna, C. N., Stevens, L. A., Meredith, W., Snape, C. E., Vane, C. H., …Carr, A. D. (2019). Shale gas reserve evaluation by laboratory pyrolysis and gas holding capacity consistent with field data. Nature Communications, 10(1), Article 3659. https://doi.org/10.1038/s41467-019-11653-4

Exploration for shale gas occurs in onshore basins, with two approaches used to predict the maximum gas in place (GIP) in the absence of production data. The first estimates adsorbed plus free gas held within pore space, and the second measures gas y... Read More about Shale gas reserve evaluation by laboratory pyrolysis and gas holding capacity consistent with field data.

Developing a sustainable route to environmentally relevant metal-organic frameworks: ultra-rapid synthesis of MFM-300(Al) using microwave heating (2019)
Journal Article
Thomas-Hillman, I., Stevens, L. A., Lange, M., Möllmer, J., Lewis, W., Dodds, C., …Laybourn, A. (2019). Developing a sustainable route to environmentally relevant metal-organic frameworks: ultra-rapid synthesis of MFM-300(Al) using microwave heating. Green Chemistry, 21(18), 5039-5045. https://doi.org/10.1039/c9gc02375e

NO2, SO2 and CO2 are major air pollutants causing significant environmental and health problems. Metal-organic frameworks (MOFs), in particular [Al2(OH)2(C16O8H6)](H2O)6 (trivial names: NOTT-300/MFM-300(Al)), have shown great promise for capturing th... Read More about Developing a sustainable route to environmentally relevant metal-organic frameworks: ultra-rapid synthesis of MFM-300(Al) using microwave heating.

Formation of Metallurgical Coke within Minutes through Coal Densification and Microwave Energy (2019)
Journal Article
Williams, O., Ure, A., Stevens, L., Binner, E., Dodds, C., Kingman, S., …Lester, E. (2019). Formation of Metallurgical Coke within Minutes through Coal Densification and Microwave Energy. Energy and Fuels, 33(7), 6817-6828. https://doi.org/10.1021/acs.energyfuels.9b00511

This paper shows how feedstock densification gives rise to a step change in the time required to create a metallurgical grade coke using microwave energy. Five densified coking and non-coking coals were heated in a multi-mode microwave 2450 MHz cavit... Read More about Formation of Metallurgical Coke within Minutes through Coal Densification and Microwave Energy.

Fast regeneration of activated carbons saturated with textile dyes: Textural, thermal and dielectric characterization (2019)
Journal Article
Durán-Jiménez, G., Stevens, L. A., Hodgins, G. R., Uguna, J., Ryan, J., Binner, E. R., & Robinson, J. P. (2019). Fast regeneration of activated carbons saturated with textile dyes: Textural, thermal and dielectric characterization. Chemical Engineering Journal, 378, Article 121774. https://doi.org/10.1016/j.cej.2019.05.135

This study presents an investigation for comparing the regeneration process of two activated carbons saturated with Basic Blue 9 (BB9) and Acid Blue 93 (AB93) using conventional (250–500 °C) and microwave heating (100–300 W). The effect of the textil... Read More about Fast regeneration of activated carbons saturated with textile dyes: Textural, thermal and dielectric characterization.

Continuous testing of silica-PEI adsorbents in a lab.-scale twin bubbling fluidized-bed system (2019)
Journal Article
Kim, J., Woo, J., Jo, S., Lee, S., Moon, J., Kim, H., …Park, Y. C. (2019). Continuous testing of silica-PEI adsorbents in a lab.-scale twin bubbling fluidized-bed system. International Journal of Greenhouse Gas Control, 82, 184-191. https://doi.org/10.1016/j.ijggc.2019.01.007

In this study, a lab.-scale twin bubbling fluidized-bed system (TBS) has been used continuously to test the performance for CO2 adsorption of silica-PEI (S.PEI) adsorbents, containing 40 wt.% of PEI, which were supplied by the University of Nottingha... Read More about Continuous testing of silica-PEI adsorbents in a lab.-scale twin bubbling fluidized-bed system.